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filingDate 1992-01-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1993-10-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7836cb5767c2f1fb4543d464e70209c2
publicationDate 1993-10-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5250737-A
titleOfInvention Process for hydrocarbyl trisulfide product
abstract A method for preparing an essentially chlorine free additive mixture for oleaginous fluids containing less than 15 wt. % dialkyl higher-polysulfides, the process comprising: a) forming a reaction mass comprising olefin, a sulfur source, and a catalyst; b) heating the reaction mass to a temperature and for a period of time which is sufficient to form a mixture of olefin, alkyl mercaptan, dialkyl disulfide, dialkyl trisulfide and dialkyl higher-polysulfides; and c) refluxing the reaction mass obtained in (b) at a temperature and for a period of time which are sufficient to convert at least a portion of the dialkyl higher-polysulfides to dialkyl trisulfide so as to obtain the additive mixture containing less than 15 wt. % dialkyl higher-polysulfides.
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