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filingDate 1990-10-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1992-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2c2cb604428dd6f90ebfddcd567171cf
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bb514717a6faecccae89be078d5f643f
publicationDate 1992-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5149889-A
titleOfInvention Composition for use in organolithium synthesis reactions
abstract A process is disclosed for the preparation of tertiary alcohols, alpha-alkyl substituted nitriles, alkyl-substituted imines or tertiary amines by alkylation of a starting material that is a carbonyl compound or a nitrile followed by hydrolysis wherein the alkylation is carried out with the aid of a reaction system formed by suspending a mixture of: n substantially 15 to 25% by weight of methyllithium or ethyllithium; n substantially 35 to 45% by weight of an inorganic compound selected from the group which consists of at least one metal oxide selected from the group which consists of SiO 2 , Al 2 O 3 , and CaO, and synthetic anhydrous aluminum silicate; and n substantially 35 to 45% by weight of a paraffin oil or wax; in an organic solvent selected from the group which consists of: n C 5 to C 10 saturated aliphatic hydrocarbons, C 5 to C 10 cycloaliphatic hydrocarbons, aromatic hydrocarbons selected from the group which consists of benzene, toluene, and xylene, and aliphatic or cycloaliphatic ethers selected from the group which consists of diisopropyl ether, di-n-butyl ether, tert-butylether, tetrahydrofuran and dioxane.
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priorityDate 1988-05-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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