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filingDate 1990-02-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1992-08-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1992-08-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5141837-A
titleOfInvention Method for preparing coating compositions containing photoconductive perylene pigments
abstract An electrophotographic coating composition comprising finely-divided photoconductive perylene pigment dispersed in a solvent solution of polymeric binder is prepared by the steps of (1) milling a perylene pigment with milling media comprising inorganic salt and non-conducting particles under shear conditions in the substantial absence of the solvent to provide pigment having a particle size up to 0.2 micrometer, (2) continuing the milling at higher shear at a temperature up to about 50° C., to achieve a perceptible color change of the pigment particles, (3) rapidly reducing the temperature of the milled pigment by at least 10° C., (4) separating the milled pigment from the media and (5) mixing the milled pigment with the solvent solution of polymeric binder to form the coating composition. A very high degree of dispersion of photoconductive perylene pigment in solvent solution of polymeric binder is achieved by this method.
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