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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B53-00
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G03C7-34
filingDate 1989-11-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1991-08-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3ff592b376175012db27f40566f008f3
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_43f3d8016ffc0ff24387856763fd148f
publicationDate 1991-08-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5041605-A
titleOfInvention Method of synthesizing phenolic cyan-dye-forming photographic couplers
abstract Phenolic cyan-dye-forming couplers characterized by a p-cyanophenylureido group in the 2-position of the phenol are synthesized in high yield by a process comprising the steps of contacting, in a reaction solvent in the presence of a transition metal catalyst at moderate temperature and atmospheric pressure, a coupler intermediate having a nitro group in the 5-position with a hydrogen donor, such as, for example, ammonium formate, to thereby form the corresponding 2-(p-cyanophenylureido)-5-aminophenol and reacting the 2-(p-cyanophenylureido)-5-aminophenol with an acylating agent to form the phenolic cyan-dye-forming coupler.
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