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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D209-48
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D207-448
filingDate 1989-04-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1991-02-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6b322ecd8b954be283b4f68fdbe5c8e4
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3e8cc77fc31bcd1576bd36cf26b604de
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publicationDate 1991-02-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4990626-A
titleOfInvention Process for preparing bisimides products
abstract In a first embodiment this invention relates to a process for preparing a white product which principally contains a bisimide. The process comprises: providing tetrabromophthalic anhydride and a solvent in a reaction vessel; forming, at a temperature within the range of from about 140° C. to about 200° C., a reaction mass by adding a diamine, a diamine salt or a mixture thereof to the solution, the formation of the reaction mass resulting in the production of a bisimide precipitate which becomes a component of the reaction mass; terminating the addition of the diamine when the molar ratio of the tetrabromophthalic anhydride initially present in the solution to the diamine or diamine salt added is substantially stoichiometric; cooking the bisimide precipitate to increase the average sphericity of the particles making up the bisimide precipitate; and recovering from the reaction mass, as the bisimide product, the cooked precipitate. In a second embodiment the cooking step is optional and the retention of water formed during the diamine or diamine salt addition is featured.
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