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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-74
filingDate 1989-04-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1990-08-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_36ee81a2fc91c39288b3fec87c525701
publicationDate 1990-08-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4948897-A
titleOfInvention Method of preparation of 2,6-bis(picrylamino)-3,5-dinitropyridine
abstract A method for preparing 2,6-bis(picrylamino)-3,5-dinitropyridine (PYX) which includes the steps of first dissolving crystalline PYX in a primary solvent in which the solvent used is selected from the group consisting of pyridine, dimethylformamide, methylsulfoxide or mixtures thereof. The primary solvent system is then combined with a second solvent in which the PYX is substantially insoluble, but which, in admixture with the primary solvent, forms a true solution of the PYX, referred to as the secondary solution. A third solvent is then added to the binary solvent system, which third solvent is soluble with the binary solvent system but which promotes precipitation of PYX in a form which exhibits improved characteristics as an explosive.
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priorityDate 1987-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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