http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4792604-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_4976a2965a6f1f78fd131ea1cd31d5ef |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D223-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D211-76 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D207-27 |
classificationIPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D207-26 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D223-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D211-76 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D- http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D211-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D207-27 |
filingDate | 1987-03-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1988-12-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b50be117ef6c677472ddf2a68ac8902a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_47ab28493261171576404c716371cd55 |
publicationDate | 1988-12-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | US-4792604-A |
titleOfInvention | Manufacture of haloalkyl lactams |
abstract | A process for the manufacture of haloalkyl lactams having the formula ##STR1## wherein n is an integer having a value of from 1 to 3; m is an integer having a value of 1 or 2 and X is chlorine or bromine in the absence of an inert solvent by reacting a hydroxyalkyl lactam of the formula ##STR2## with a thionyl chloride or bromide in the liquid phase under anhydrous conditions, vaporizing and removing any excess thionyl halide along with SO 2 by-product from the liquid reaction mixture under vacuum followed by vacuum distillation of the remaining liquid product mixture at a temperature below its decomposition and recovering said product. n The product of this process can be obtained in greater than 90% yield and 99% purity. |
priorityDate | 1987-03-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 57.