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filingDate 1987-03-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1988-12-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b50be117ef6c677472ddf2a68ac8902a
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publicationDate 1988-12-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4792604-A
titleOfInvention Manufacture of haloalkyl lactams
abstract A process for the manufacture of haloalkyl lactams having the formula ##STR1## wherein n is an integer having a value of from 1 to 3; m is an integer having a value of 1 or 2 and X is chlorine or bromine in the absence of an inert solvent by reacting a hydroxyalkyl lactam of the formula ##STR2## with a thionyl chloride or bromide in the liquid phase under anhydrous conditions, vaporizing and removing any excess thionyl halide along with SO 2 by-product from the liquid reaction mixture under vacuum followed by vacuum distillation of the remaining liquid product mixture at a temperature below its decomposition and recovering said product. n The product of this process can be obtained in greater than 90% yield and 99% purity.
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