Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_e899199238cd97bdebfa84869ece733b |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-5077 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-94 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-90 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-66 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-92 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-50 |
filingDate |
1985-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
1986-10-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_de2daed13e2b17682eae4dbf292a2954 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4fef83301a9b12efb5b4520b76bfaf8c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_09e8857dc54afcee59297a743fb67bc1 |
publicationDate |
1986-10-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
US-4618720-A |
titleOfInvention |
Preparation of alkyldiarylphosphines |
abstract |
An improved process is disclosed for preparing alkyldiarylphosphines and related compounds. Typically, diphenylphosphinous chloride is reacted in solution with an excess of an alkali metal; and the reaction product reacted with chlorohexane thereby forming hexyldiphenylphosphine. The improved process obtains greater yields, by use of critical amounts of alkali metal; use of a single reactor rather than two reactors; preinitiation of the first stage reaction; reduction of temperatures to increase reaction rate under certain conditions; and preferred reactants and physical form thereof. Novel products include behenyldiphenylphosphine. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5710340-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5777169-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5550295-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6563005-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5527967-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5654485-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5654486-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5866720-A |
priorityDate |
1985-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |