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filingDate 1985-05-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1986-08-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_78fc884685f16bcc1a0e496301a2489c
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publicationDate 1986-08-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4608127-A
titleOfInvention Dibenzofuran distillation and crystallization process
abstract Separation and recovery of dibenzofuran of high purity is accomplished by distilling a coal tar fraction having boiling point range of 220 DEG to 300 DEG C. thereby producing a dibenzofuran fraction having a dibenzofuran content of not less than 30% by weight, a dibenzofuran/acenaphthene molar ratio of not less than 1.3, and a fluorene/dibenzofuran molar ratio of not more than 0.05, then introducing the dibenzofuran fraction obtained as described above into a continuous crystallization purification unit provided with a cooling zone for crystallization of the feed, a heating zone for melting the purified crystals, and a refining zone for enabling crystals being transferred from said cooling zone to said heating zone to come into counter current contact with a mass of molten crystals midway along the path between said two zones, and subjecting the dibenzofuran fraction to continuous crystallization purification therein.
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priorityDate 1980-12-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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