Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_5c24684033fba97d1ad845ce453a57e3 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-02 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-755 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-43 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B61-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-74 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02 |
filingDate |
1984-05-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
1985-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3f7976c69fa226f6d47948821baf993f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_13bfe7fe3ef56b8e213d78e3d4cdca76 |
publicationDate |
1985-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
US-4540816-A |
titleOfInvention |
Single-vessel process for preparing ring-substituted n-alkylanilines |
abstract |
Process for preparing ring-substituted N-alkylanilines of the formula (1) ##STR1## in which R 1 and R 2 each denote methyl or ethyl, in a single vessel, which comprises acylating m-nitroaniline in an excess of an aliphatic carbonyl compound of the formula (2) ##STR2## in which R 1 is as defined above, with an acylating agent which contains the --CO--R 2 acyl radical--which is transferred-- and reductively alkylating the resulting compound of the formula (3) ##STR3## in which R 2 is as defined above, at temperatures of 120°-160° C. under a hydrogen pressure of 20-150 bar without intermediate isolation through the presence of an acid reaction promoter and of a nickel catalyst. |
priorityDate |
1983-05-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |