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filingDate 1984-03-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1985-02-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_37f806c113f97fdd0194a63ebc777d8c
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publicationDate 1985-02-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4497697-A
titleOfInvention Electrolytic preparation of 3,6-dichloropicolinic acid
abstract The rate of production of 3,6-dichloropicolinic acid by reduction of tetrachloropicolinic acid in basic aqueous solution in a given cell can be considerably increased if a trichloropicolinic acid is added to the tetrachloropicolinic acid feed in substantially greater proportions than can result from in-situ reduction of the tetrachloro acid. Preferably, the trichloro acid is obtained by acid hydrolysis of by-products of symmetrical tetrachloropyridine manufacture by chlorination/chlorinolysis of 6-chloro-2-(trichloromethyl)pyridine.
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