http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4427603-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_5c24684033fba97d1ad845ce453a57e3 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-425 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-42 |
filingDate | 1982-05-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1984-01-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5234d085a83606dcc95c345daa6ea2ce http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_21b7f9ef276a7c175cddacb70e06bd80 |
publicationDate | 1984-01-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | US-4427603-A |
titleOfInvention | Process for making phosphonic acid ester chlorides |
abstract | The disclosure relates to a process for making phosphonic acid ester chlorides of the general formula (I) n n R--P(O) ClOR' (I) n n in which R stands for an alkyl group with 1 to 6 carbon atoms or an aryl group and R' stands for an alkyl group with 1 to 20 carbon atoms or an aryl group. More particularly, a compound of general formula (II) n n R--PCl.sub.2 (II) n n is reacted with a sulfuric acid monoester of general formula (III) n n R'--O--SO.sub.3 H (III) n n R and R' in formulae (II) and (III) having the meanings given above; the reactants are used in about equimolar proportions and the reaction is effected at a temperature of from -20° C. to 50° C. After termination of the reaction, the phosphonic acid ester chloride is separated from the reaction mixture by subjecting this latter to distillation under vacuum. |
priorityDate | 1981-05-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 49.