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filingDate 1982-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1983-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1983-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4401826-A
titleOfInvention Method for production of mercapto functional silanes
abstract An improved method for the production of mercapto functional silanes is provided whereby reactions between haloalkyl silanes and thioureido compounds in the presence of ammonia are accelerated with tertiary nitrogen-containing compounds. In a preferred embodiment the reaction of 3-chloropropyltrimethoxysilane with thiourea is accelerated by N,N-dimethylformamide and other compounds to produce 3-mercaptopropyltrimethoxysilane at lower temperatures and with increased yield.
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