http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4374108-A

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filingDate 1980-11-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1983-02-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b352fe5999b99c8d0dfbc7ce04d8580f
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4c6b7020255b125740e7d79bdb5c0a3a
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publicationDate 1983-02-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4374108-A
titleOfInvention Process of preparing alkali monofluorophosphate
abstract An alkali monofluorophosphate expressed by the formula M 2 PO 3 F, where M represents Na or K, can readily be synthesized under a relatively mild reaction condition by making HF gas contact with powdery or fine granular M 4 P 2 O 7 or M 2 HPO 4 placed in a reaction vessel and maintained at a temperature in the range from about 200° C. to about 450° C., and more preferably in the range of 280°-360° C. It is suitable to make HF gas continuously flow into and pass through the reaction vessel until the total quantity of HF flowed into the vessel amounts to 100 to 150% of the theoretical value for conversion of M 4 P 2 O 7 or M 2 HPO 4 to M 2 PO 3 F.
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priorityDate 1979-11-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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