http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4348529-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_08e5126e16ad1c7aae67ba760e92e943 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D339-08 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D339-08 |
filingDate | 1981-08-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1982-09-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6af3771a4f1b4523a607c16464ac9722 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5c3517335f0c7acdefccec9c96f53fbc http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e1628aa458f5a7e56febf6e68fc3d3f5 |
publicationDate | 1982-09-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | US-4348529-A |
titleOfInvention | Synthesis of cyclic disulfone compounds |
abstract | This invention relates to a method of synthesizing bis-sulfones of the formula <IMAGE> wherein R1 and R2 each are hydrogen, alkyl, phenalkyl, phenyl or phenyl-substituted with an electron-donating or electron-withdrawing group and n is an integer 2, 3 or 4 (a) by reacting a 1,3-dithio compound with n-butyllithium to generate the anion of said compound, (b) reacting said anion with a carbonyl compound to give the 2-substituted carbonol anion intermediate, (c) reacting said intermediate with an acyl chloride or a chloroformate to give the corresponding ester, and (d) reacting said ester with a peracid to give the bis-sulfone product. The subject invention also is concerned with the novel intermediates of step (c). |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5098928-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4469877-A |
priorityDate | 1981-08-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 46.