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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D213-16
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D319-12
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-16
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D319-12
filingDate 1979-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1981-08-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_808d121e27066e373db0f9d4e2fb1200
publicationDate 1981-08-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4283339-A
titleOfInvention Preparation of dioxane and co-products
abstract Dioxane is prepared by reaction of polyethylene glycols in a catalytically active liquid reaction medium comprising a mixture of partial phosphate esters of a polyethylene glycol, and ammonium salts of partial esters of a polyethylene glycol. Along with dioxane, valuable co-products, including the compound 5-ethyl-2-methylpyridine, are formed from which the dioxane is readily separated in highly pure form. The catalytically active liquid reaction medium is derived from the reaction of ammonium dihydrogen phosphate with a polyethylene glycol at temperatures preferably in the range from 190° to 225° C. Temperatures of reaction between the polyethylene glycol and the catalytically active liquid reaction medium to form the dioxane and co-products are preferably in the range of from about 225° C. to about 275° C.
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4405799-A
priorityDate 1979-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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