| abstract |
Reaction mother liquor of terephthalic acid production is treated to separate volatile component mainly composed of acetic acid and solid components composed of used catalyst or heavy metal salt(s), residual terephthalic acid and reaction by-products by using combination of a tubular type heater having at least one heating tube of a relatively small diameter and a separation chamber in which the heating tube(s) open(s) at one end thereof. |