http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4150057-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_2a6a9431aa1fe5109ca95ad4e332231b |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F5-022 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F5-02 |
filingDate | 1978-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1979-04-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d47e195b65dc7d5968d5ad7131a4d4e2 |
publicationDate | 1979-04-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | US-4150057-A |
titleOfInvention | Method for preparation of a carboranyl burning rate accelerator precursor |
abstract | Disclosed is a method of synthesis and the compound synthesized B10H12[(CH3)2S]2. The method employs the starting compound (R4N)2B10H10, as a source of the ten-boron ion (e.g., B10H10-2), in which the starting compound, wherein R equals an alkyl with the formula CnH2n+1 and wherein n equals 2, 3, or 4, is converted to Li2B10H10 by ion-exchange. The Li2B10H10 is reacted with HCl in (CH3)2S solution to produce the compound B10H12[(CH3)2S]2, a precursor compound for synthesizing carboranyl burning rate accelerators. The precursor compound is reacted with propargyl propionate if the interest is to synthesize carboranylmethyl propionate; 1-octyne to synthesize n-hexylcarborane; or propargyl ethyl sulfide or propargyl propyl sulfide to synthesize carboranylmethyl ethyl sulfide or carboranylmethyl propyl sulfide, respectively. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103288097-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103288097-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-9598352-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6143264-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-10679759-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2014197076-A2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-101031504-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104017010-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102558206-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-10886032-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104017010-B |
priorityDate | 1978-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 126.