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filingDate 1976-04-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1978-09-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1978-09-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4113786-A
titleOfInvention Hydrogen chloride recovery
abstract Process for recovering hydrogen chloride from a gas withdrawn from an oxychlorination reaction zone which contains hydrogen chloride and water vapor wherein the gas is initially cooled, followed by contacting the gas with a small amount of water to absorb the hydrogen chloride from the gas. The water content is controlled to provide an aqueous hydrogen chloride stream having a hydrogen chloride concentration of from 10% to 20%, with the absorbed aqueous hydrogen chloride being recycled to the oxychlorination reaction. A dilute aqueous hydrogen chloride stream, obtained from another portion of the process, may be employed in the initial cooling step, as a direct quench, resulting in vaporization of the dilute aqueous hydrogen chloride stream and eliminating the necessity for a hydrogen chloride concentrator.
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