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filingDate 1976-09-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1977-12-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1977-12-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4065267-A
titleOfInvention Manufacture of alkylated urea or melamine formaldehyde with in-process alcohol recovery
abstract This invention relates to an improved apparatus for preparing alkylated urea or melamine formaldehyde resins from alcohols having a boiling point higher than water, which apparatus permits the return of substantially dry alcohol from the water distillation system to the reactor. n The apparatus comprises a reactor connected to a fractionating column, having a rectifying section above a stripping section, at the junction of the rectifying section and the stripping section; a reboiler at the bottom of the fractionating column, which returns substantially dry alcohol to the reactor; a condenser which condenses the alcohol-water vapor mixture exiting the rectifying section of the column; and a separator device which separates the condensed mixture into an alcohol phase and a water phase, and from which the alcohol phase is returned to the top portion of the column. n Use of the apparatus of the invention results in a substantial reduction in reaction times.
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priorityDate 1975-01-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 46.