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filingDate 1976-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1977-08-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1977-08-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4039347-A
titleOfInvention Method of preparing zinc orthotitanate pigment
abstract Zinc orthotitanate (Zn 2 TiO 4 ) suitable for use as a pigment for spacecraft thermal control coatings is prepared by heating a slightly zinc-deficient reaction mixture of precipitated oxalates of zinc and titanium. The reaction mixture can be formed by co-precipitation of zinc and titanium oxalates from chloride solution or by mixing separately precipitated oxalates. The mixture is first heated to 400° to 600° C to remove volatiles and is then rapidly heated at 900° to 1200° C. Zinc orthotitanate produced by this method exhibits the very fine particle size needed for thermal control coatings as well as stability in a space environment.
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