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filingDate 1974-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1976-09-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aa5bc92aca85c7015c84cbbf00cb9d7d
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publicationDate 1976-09-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-3979372-A
titleOfInvention Preparation of titanium trichloride polymerization catalyst component
abstract It is known to prepare highly active catalyst components for a Ziegler polymerization catalyst by reduction of titanium tetrachloride with an aluminum alkyl. An improvement in the preparation of such catalysts which leads to production of highly sterospecific as well as highly active catalyst components consists of including in the preparation the step of washing the reaction mixture which contains the desired TiCl3 composition with an aliphatic hydrocarbon at temperatures above 40 DEG C and separating the washed solids from the wash liquid at a temperature above 40 DEG C. A heat treatment above 80 DEG C precedes, accompanies, or follows the washing and separation step. The washing step may be carried out in a single or in multiple stages.
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