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filingDate 1975-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1976-05-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4f4dc392edac597e4b4a0027893854d3
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publicationDate 1976-05-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-3954895-A
titleOfInvention Method of separating and recovering alkenylbenzenes and unreacted alkylbenzenes from the alkenylation reaction product
abstract In the method wherein an alkenylation reaction product liquid obtained by the alkenylation reaction of an alkylbenzene and a C4 - C5 conjugated diene in the presence of alkali metal catalysts and containing unreacted alkylbenzene, alkali metal catalysts and organo-alkalimetal compounds is conveyed to a distillation zone at which said alkenylation reaction product liquid is separated by distillation to recover an alkenylbenzene-containing fraction and an unreacted alkylbenzene-containing fraction, the improvement which comprises adjusting the total of the concentrations of said alkali metal catalysts and organo-alkalimetal compounds in said alkenylation reaction product liquid introduced to the distillation zone so as to be 0.09 - 15 milligram atoms per kilogram of said product liquid, calculated as alkalimetal atoms, and thereafter conducting the distillation of said product liquid under conditions of non-addition of alcohols.
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