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filingDate 1974-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1975-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d516d15c06b690a0598fedcf192df4ce
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publicationDate 1975-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-3890288-A
titleOfInvention Process for making poly-alpha-oxyacrylic acid and its alkali metal salts
abstract Production of poly- Alpha -oxyacrylic acid by contacting a solution of Alpha -chloracrylic acid with one or more radicalyielding polymerization catalysts, heating and thereby hydrolyzing the resulting poly- Alpha -chloracrylic acid in queous solution with the resultant precipitation of solid polyAlpha -oxyacrylic acid and separating the poly- Alpha -oxyacrylic acid. More particularly, and aqueous Alpha -chloracrylic acid solution is contacted with the radical-yielding polymerization catalysts for a period of at least 30 minutes and, while leaving the resulting poly- Alpha -chloracrylic acid unseparated, it is heated for a period of at least 1 hour to temperatures within the range 80* and 110*C.
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