http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-3869545-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_af99df08b153738cd418446a75d09bfc |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B6-06 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B6-06 |
filingDate | 1964-03-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1975-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5e6310edafe24b2db90acca60e31fe48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8a97b3dd2420fcde14e71c3152dc00a2 |
publicationDate | 1975-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | US-3869545-A |
titleOfInvention | Preparation of aluminum hydride |
abstract | 1. In a process for preparing aluminum hydride by reacting an alkali metal aluminum hydride with aluminum chloride in an aliphatic ether solution the improvement which comprises; providing as the alkali metal aluminum hydride reactant a mixture of sodium aluminum hydride and lithium aluminum hydride in an aliphatic ether, the molar proportions of said sodium aluminum hydride-lithium aluminum hydride being about 5/1 to about 1/1, adding to said mixture over a period of from about 5 seconds to about 40 minutes while maintaining the reaction temperature below the boiling point of the ether aluminum chloride in an amount at a maximum of about 10 weight percent in excess of that required for stoichiometric reaction with said sodium aluminum hydride thereby to prepare aluminum hydride and co-precipitated inorganic halides and other impurities, dissolving said aluminum hydride in aliphatic ether solvent thereby freeing said aluminum hydride product from said co-precipitated inorganic halides and other impurities, and removing the co-precipitated solids from said aluminum hydride product solution. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-9228267-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6617064-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-9676625-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6228338-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-10246785-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-9327974-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-10435297-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-10233079-B2 |
priorityDate | 1964-03-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 42.