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filingDate 1964-03-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1975-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5e6310edafe24b2db90acca60e31fe48
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8a97b3dd2420fcde14e71c3152dc00a2
publicationDate 1975-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-3869545-A
titleOfInvention Preparation of aluminum hydride
abstract 1. In a process for preparing aluminum hydride by reacting an alkali metal aluminum hydride with aluminum chloride in an aliphatic ether solution the improvement which comprises; providing as the alkali metal aluminum hydride reactant a mixture of sodium aluminum hydride and lithium aluminum hydride in an aliphatic ether, the molar proportions of said sodium aluminum hydride-lithium aluminum hydride being about 5/1 to about 1/1, adding to said mixture over a period of from about 5 seconds to about 40 minutes while maintaining the reaction temperature below the boiling point of the ether aluminum chloride in an amount at a maximum of about 10 weight percent in excess of that required for stoichiometric reaction with said sodium aluminum hydride thereby to prepare aluminum hydride and co-precipitated inorganic halides and other impurities, dissolving said aluminum hydride in aliphatic ether solvent thereby freeing said aluminum hydride product from said co-precipitated inorganic halides and other impurities, and removing the co-precipitated solids from said aluminum hydride product solution.
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priorityDate 1964-03-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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