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publicationDate 2022-10-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2022315445-A1
titleOfInvention Preparation method for 2-4 micrometers battery-grade cobalt tetroxide
abstract The present invention discloses a preparation method for 2-4 μm battery-grade cobalt tetroxide, comprises following steps: 1) adding a cobalt salt solution and an alkaline solution by parallel flows to a reactor with a base solution and an air flow, controlling pH value of a system by adjusting flow rate of the alkaline solution for coprecipitation reaction at a certain stirring rate, decreasing the pH value of the reaction system and increasing flow rate of the cobalt salt solution after the reaction solutions begin to overflow; 2) aging and drying the cobalt oxyhydroxide slurry in sequence; 3) calcining the dried cobalt oxyhydroxide. By adopting this method, tap density of the battery-grade cobalt tetroxide obtained is much higher than that of cobalt tetroxide with a same particle size specification prepared by the prior art.
priorityDate 2019-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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