http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2018230078-A1

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filingDate 2016-07-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_266e70684df1880e3fc82eb6816cf815
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publicationDate 2018-08-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2018230078-A1
titleOfInvention Method for producing high-purity terephthalic acid
abstract A method for producing high-purity terephthalic acid, comprising following steps (a) to (c):n the step (a); obtaining crude terephthalic acid crystal by liquid phase-oxidizing a p-phenylene compound; the step (b); obtaining a terephthalic acid crystal slurry by a catalytic hydrogenation treatment of the crude terephthalic acid crystal; and the step (c); introducing the terephthalic acid crystal slurry into an upper portion of a mother liquor replacement tower, and bringing the slurry into contact with an upward flow of replacement water introduced from a bottom portion of the mother liquor replacement tower while making the terephthalic acid crystal settled down in the tower, and extracting the terephthalic acid crystal as a slurry with the replacement water from the tower bottom portion, wherein (1) a stirring blade unit is disposed in a slurry layer in the bottom portion of the mother liquor replacement tower, and fluidity of the slurry layer is maintained by rotating the stirring blade unit in such a way that stirring power is 0.1 to 1.0 kWh/m 3 per unit volume of the slurry layer, and (2) the replacement water is fed through the replacement water feed opening provided in the stirring blade unit.
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