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filingDate 2016-06-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2018-07-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2018185810-A1
titleOfInvention A high-throughput combinatorial materials experimental apparatus for in-situ synthesis and real-time characterization and related methods
abstract A high-throughput combinatorial materials experimental apparatus for in-situ synthesis and real-time characterization includes a composition spread device to prepare continuous or discrete composition distribution as precursor of the high-throughput experimental samples library, a low temperature diffusion mixing device to thoroughly mix the composition spread in the thickness direction through diffusion at a relatively low temperature to form an amorphous precursor, and an integrated synthesis-characterization unit for heat treatment of the material library precursor in either a parallel or point-by-point scanning mode at different thermodynamic conditions for phase formation and to characterize features or properties of the materials of interest in an in-situ and real-time manner. The integrated synthesis-characterization unit includes a chamber maintained at desired vacuum and atmosphere, a micro-heating source, an excitation source, a signal collector, and a sample holder.
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priorityDate 2015-06-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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