http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2017233425-A1

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filingDate 2014-12-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5e5dd2d0d2182986819344a3eb6df6e8
publicationDate 2017-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2017233425-A1
titleOfInvention The chemical synthesis method of phillyrin
abstract The present invention relates to a chemical synthesis method for phillyrin. The method of the present invention comprises: first dissolving a glycosyl receptor phillygenin and a glycosyl donor in an organic solvent for glycosylation to obtain tetraacyl phillyrin; then dissolving the tetraacyl phillyrin in a second organic solvent, and adding sodium methoxide for deacylation, adding an acidic pH regulator to regulate the pH value of the reaction mixture to neutral; and finally carrying out purification treatment to obtain phillyrin. The advantages and practical values of the chemical synthesis method for phillyrin of the present invention lie in: the raw material is easy to get, the catalysts used for glycosylation are cheap and easy to get, the production cost is greatly reduced, and it can be used for industrial production.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110642906-A
priorityDate 2014-08-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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