http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2016032427-A1

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filingDate 2014-09-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_178fb715fe82ea8b8fa8d596a08df582
publicationDate 2016-02-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2016032427-A1
titleOfInvention Method for manufacturing high purity manganese and high purity manganese
abstract The present invention relates to a method for manufacturing a high purity Mn, the method comprising: placing a Mn raw material in a magnesia crucible to perform melting with the use of a vacuum induction melting furnace (VIM furnace) at a melting temperature of 1240 to 1400° C. under an inert atmosphere of 500 Torr or less; then adding calcium in a range between 0.5 and 2.0% of the weight of Mn to perform deoxidation and desulfurization; casting the resultant in an iron mold after the completion of the deoxidation and desulfurization to manufacture an ingot; then placing the Mn ingot in a skull melting furnace; reducing pressure to 10 −5 Torr or less with a vacuum pump; starting heating and keeping the Mn in a molten state for 10 to 60 minutes; and then ending the melting reaction for obtaining a high purity metal Mn. Provided is a method for manufacturing a high purity metal Mn from a commercially available electrolytic Mn. In particular, an object is to obtain a high purity metal Mn in which the amount of impurities such as B, Mg, Al and Si is small.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113088828-A
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