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filingDate 2012-10-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8a527c9f2701bbdf012f2c623cad9bcf
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d4375f24255ad73ebacc7da7e4ad0990
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publicationDate 2014-09-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2014288322-A1
titleOfInvention Preventing Solvent of Crystallization in Production of Polyphosphite Ligands
abstract Residual wash solvent, e.g., ethyl acetate, is removed from polyphosphite, e.g., bisphosphite, crystals by a process comprising the steps of: A. Mixing the polyphosphite crystals and residual wash solvent with a secondary alcohol, e.g., isopropyl alcohol (IPA), to form a mixture of polyphosphite crystals, residual wash solvent and secondary alcohol, and B. Drying the mixture to remove the residual wash solvent and secondary alcohol to a content of less than 0.5 wt % based on the weight of the polyphosphite crystals.
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