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publicationDate 2014-08-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2014235801-A1
titleOfInvention Polyisobutylene Prepared at High Velocity and Circulation Rate
abstract A method of making a polyisobutylene polymer in a recirculating loop reactor with one or more reaction tubes in contact with a heat transfer medium includes controlling the delta P and polymerization reaction to provide a linear velocity of the reaction mixture of at least 11 ft/sec in the one or more tubes of the loop reactor and/or controlling the delta P and polymerization reaction of steps (b) and (c) to provide a recirculation ratio of the recirculation rate to the feed rate of at least 30:1. Typically, the process utilizes a recirculating pump operating at a pressure differential of from 35 psi to 70 psi.
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