Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_79f633062b4b63e578ac1c4cc6f9dd57 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b7317808024e524eea40a6c5a5ad6a22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b6e88ada956151edaf69855a9cbb9fed |
classificationCPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y10T428-2989 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y10S977-896 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2006-42 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B82Y40-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2002-82 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2004-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2004-64 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C51-412 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F15-025 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B82Y30-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01G49-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01G49-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01G49-08 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G49-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F15-02 |
filingDate |
2011-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e53654f8be4901b97826848758cd1a96 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9b2986026da4b72c7206b32698f560c0 |
publicationDate |
2013-04-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
US-2013089740-A1 |
titleOfInvention |
Synthesis and use of iron oleate |
abstract |
The present invention relates to a method of forming an iron oleate complex comprising the steps of: (a) dissolving an oleate in a low-order alcohol solvent at a temperature of about 35° C. to 65° C.; (b) adding a non-polar solvent to the solution of step (a); (c) adding an iron salt dissolved in a low-order alcohol to the solution of step (b); (d) agitating the solution of step (c) at a temperature of about 50° C. for at least 5 min; (e) cooling the reaction mixture of step (d) to a temperature of about 15° C. to 30° C.; (f) optionally filtering the reaction mixture of step (e); (g) separating the non-polar solvent phase from the low-order alcohol phase; (h) washing and drying the non-polar solvent phase; (i) removing volatiles from the non-polar solvent phase of step (h) by evaporation; and (j) mixing the product of step (i) with a polar solvent to yield a solid iron oleate complex. The present invention further relates to an iron oleate complex obtainable by the method of the invention, an iron oleate complex of formula I, the use of the iron oleate complex of the invention as precursor for the preparation of nanoparticles, and a method of forming iron oxide nanoparticles comprising the suspension of iron oxide/hydroxide and the iron oleate complex of the invention. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2015118390-A3 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-9153367-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2016136307-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2017210773-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113304270-A |
priorityDate |
2010-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |