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publicationDate 2012-11-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2012279111-A1
titleOfInvention Continuous process for producing biodiesel fuel
abstract A continuous process for producing biodiesel fuel with a conversion of triglycerides in biodiesel above 99.90% by weight in the transesterification step, which comprises the following steps: n a) providing a triglyceride source at a triglyceride concentration above 99.0% by weight; n b) subjecting triglycerides to a transesterification reaction with methanol, ethanol, or the mixtures thereof, at a molar ratio of triglycerides:alcohol 1:3-3.5, in the presence of 0.7 to 1.0% by weight of sodium or potassium hydroxide as catalyst, under ultrasonic cavitation conditions in an ultrasonic cavitation reactor with 2 to 8 serial cavitation cells, at a temperature of 45 to 60° C., at a pressure of 1.5 to 2 MPa (15-20 atm) and during a period of time of 15 to 30 seconds; n c) recovering the product of step b) and subjecting it to mechanical agitation operation, at a temperature of 45 to 60° C. for a maximum of 10 minutes, up to the completion of the transesterification reaction, thus obtaining a conversion of triglycerides in biodiesel above 99.90% by weight; n d) decanting and/or centrifuging the product resulting from step c) to remove glycerin; n e) purifying biodiesel obtained in step d) by exchange resins; and n f) removing by distillation methanol and water from the product of step e) and recovering the biodiesel fuel thus obtained.
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