http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2010094038-A1
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_1da521f27baffc7ec053e6bcb29002e9 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C303-26 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C303-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C309-10 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C303-24 |
filingDate | 2008-01-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_09de93e831cce49f5804b14414210c83 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0e10331d8c797b642e16867b02cd4de0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3cee20be403fd75cff4b82891c1d3898 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_84528db90778c64dc376832695fc7e31 |
publicationDate | 2010-04-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | US-2010094038-A1 |
titleOfInvention | Synthesis |
abstract | The present invention provides a method of preparing a sulfonyl ether comprising the steps of: v) reacting a sulfonic acid with an anhydride, under continuous vacuum distillation conditions, to form a carboxysulfonate; vi) reacting the carboxysulfonate with an optionally substituted cycloalkane ring containing at least 3 heteroatoms to form a sulfonyl ether pre-mix comprising a sulfonyl ether and at least two additional reaction products each containing at least one ether linkage; vii) subjecting the pre-mix to continuous vacuum distillation conditions to remove at least some of the additional reaction products from the sulfonyl ether pre-mix to provide a crude sulfonyl ether product; and viii) purifying the crude sulfonyl ether product. |
priorityDate | 2007-01-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 98.