http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2009209766-A1

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filingDate 2009-01-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2009-08-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2009209766-A1
titleOfInvention Process for the preparation of 4-amino-2,2,6,6-tetramethylpiperidine
abstract 4-amino-2,2,6,6-tetramethylpiperidine is prepared by reacting 2,2,6,6-tetramethylpiperidine-4-one with ammonia and hydrogen in the presence of nickel and/or cobalt catalyst and water. The main reaction is carried out at a pressure of at most 50 bar and a temperature of at most 120° C. up to a conversion of the 2,2,6,6-tetramethylpiperidine-4-one of at least 80%. Then, an after-reaction takes place at a higher temperature and at a higher pressure compared to the pressure and temperature of the main reaction.
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