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filingDate 2004-11-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_af130d618dd18cd1272e280aa6a431fe
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publicationDate 2009-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2009069602-A1
titleOfInvention Process for Producing 2,2'-Bis(Trifluoromethyl)-4,4'-Diaminobiphenyl
abstract A process for producing 2,2′-bis (trifluoromethyl)-4,4′-diaminobiphenyl which is useful as a raw material for polyimide resin, etc. n In benzidine rearrangement of 3,3′-bis(trifluoromethyl) hydrazobenzene in the presence of an inorganic acid such as sulfuric acid aqueous solution or concentrated hydrochloric acid, use of a water-immiscible organic solvent such as toluene as reaction solvent can increase the yield of the product. n 3,3′-bis(trifluoromethyl) hydrazobenzene can be synthesized by reduction of m-nitrobenzotrifluoride.
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