http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2004044259-A1

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filingDate 2002-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_374ee5ca3dbc344615580c17e5d61ef7
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publicationDate 2004-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2004044259-A1
titleOfInvention Process for producing propargyl bromide
abstract This invention provides a process of producing propargyl bromide in the absence of abase. The process comprises: n A) bringing together in a reaction zone under an inert atmosphere and in the absence of a base and in the presence of an inert diluent, a feed of phosphorus tribromide and a separate feed of propargyl alcohol thereby forming a reaction mixture; n B) while mechanically agitating the mixture being formed in A), maintaining the temperature of the mixture in the range of about 0° C. to about 25° C. to form a product mixture, and then n C) raising the temperature of the product mixture to a temperature in the range of about 40° C. to about 60° C. while stirring the product mixture for a ride period of at least about 2.5 hours. n Such process can be conducted as a batch process, as a semi-batch process, or as a continuous process.
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type http://data.epo.org/linked-data/def/patent/Publication

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