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filingDate 2003-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2004-02-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2004033883-A1
titleOfInvention SiA1ON containing ytterbium and method of making
abstract A SiAlON ceramic body made from a starting powder mixture that includes silicon nitride powder, and one or more powders that provide aluminum, oxygen, nitrogen and ytterbium to the SiAlON ceramic. The SiAlON ceramic body includes a two phase composite comprising alpha prime SiAlON phase, which is present in an amount greater than or equal to about 20 weight percent of the two phase composite, and a beta prime SiAlON phase wherein the alpha prime SiAlON phase containing ytterbium therein. The starting silicon nitride powder contains less than or equal to about 1.6 weight percent beta-silicon nitride. The ceramic body further includes an intergranular phase that includes an intergranular crystalline phase comprising at least one of YbAG and J-phase. The overall composition of the ceramic body is Yb a Si b Al c O d N e , wherein when a is less than 0.05, The relative intensity of the peak associated with either one or both intergranular crystalline phases of YbAG and J-phase is greater than about 2.5 of the major peak of the two-phase composite.
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