http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2003055228-A1

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filingDate 2002-08-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e5bdac514cc1f5446340ae753b94d207
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publicationDate 2003-03-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-2003055228-A1
titleOfInvention High-purity lanthanum isopropoxide and a process for producing the same
abstract The invention provides true La(OiPr) 3 preferable as a starting material for an asymmetric synthesis catalyst and a process for producing the same. In this process, anhydrous lanthanum chloride LaCl 3 is reacted with potassium isopropoxide K(OiPr) in a mixed solvent of isopropanol and toluene, then the isopropanol is distilled away to replace all the solvent by toluene, then the reaction solution is left, decanted and filtered to give a transparent filtrate, and the solvent is distilled away from the filtrate which is then vacuum-dried under heating, whereby high-purity La(OiPr) 3 is obtained in 77% yield. In this high-purity La(OiPr) 3 , the La content is 97 to 103% of the theoretical content, impurity K is 0.3% or less, (Li+Na) is 0.01% or less, Cl is 0.2% or less, and the degree of association thereof is 5.5 to 6.5.
priorityDate 2001-09-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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