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filingDate 2020-10-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-05-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_19de6b5715a61db0b23d8b8b0b1e1258
publicationDate 2021-05-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-11001553-B1
titleOfInvention Process for the synthesis of 2-nitratoethyl acrylate (2NEA)
abstract An elegant process for the synthesis of 2-nitratoethyl acrylate is a single reactive step. A 2-hydroxyethyl acrylate having only one hydroxyl group is nitrated in a 1:1 volumetric mixture of nitric acid and sulfuric acid therein forming 2-nitratoethyl acrylate. The 2-nitratoethyl acrylate is minimally soluble in a quenched cold acid water mixture, which enables relatively easy isolation of about 96% purity 2-nitratoethyl acrylate at a yield of about 85%.
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