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filingDate 2014-06-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-11-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b14b2f037e959f7f2caaae691239b8e3
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publicationDate 2020-11-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-10840491-B2
titleOfInvention Process for producing cellulose-nanofiber-filled microporous stretched polyolefin film, microporous cellulose-nanofiber composite film, and separator for non-aqueous secondary battery
abstract A method for producing a cellulose nanofiber-containing polyolefin microporous stretched film according to the invention includes: a first step of obtaining a cellulose powder dispersion mixture by uniformly dispersing a cellulose which has a powder particle shape and whose hydroxyl groups have been subjected to a lipophilizing treatment using a dibasic acid anhydride, in a plasticizer; a second step of melt-kneading the cellulose powder dispersion mixture and a polyolefin to obtain a polyolefin resin composition; a third step of extrusion-molding the polyolefin resin composition to obtain an extrudate; a fourth step of stretching the extrudate with a film stretcher to obtain a film; a fifth step of extracting out the plasticizer from the film; and a sixth step of thermally fixing the film from which the plasticizer has been extracted out for inhibiting contraction, while stretching the film at a temperature not higher than a melting point of the polyolefin, in which a twin-screw kneading extruder is used only once throughout the second and third steps.
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