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publicationDate 2019-07-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-10361075-B2
titleOfInvention Process and apparatus for measuring an organic solid sample by glow discharge spectrometry
abstract A system and a process for measuring, by glow discharge spectrometry, the elemental and/or molecular chemical composition of an organic solid sample ( 10 ). The sample ( 10 ) is positioned so as to seal a glow discharge plasma reactor ( 2 ), a gaseous mixture including at least one inert gas and gaseous oxygen is injected into the reactor ( 2 ), the concentration of gaseous oxygen being between 0.1% and 15% by weight of the gaseous mixture, an electric discharge of radiofrequency type is applied to the electrodes of the plasma reactor ( 2 ) in order to generate a glow discharge plasma, and the solid sample ( 10 ) is exposed to the plasma so as to etch an erosion crater in the solid sample ( 10 ); at least one signal representative of an ionized species of negative charge is selected and measured using a mass spectrometer ( 4 ).
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