http://rdf.ncbi.nlm.nih.gov/pubchem/patent/UA-115207-U
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C30B11-00 |
filingDate | 2016-10-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | UA-115207-U |
titleOfInvention | METHOD OF OBTAINING TlPb2BrI4 MONO CRYSTALS |
abstract | The method of obtaining halogen-containing single crystals TLRb2BrI4 involves the Assembly of the charge of the calculated quantities purified by repeated zone melting and directional crystallization at the installation intended for the implementation of the Bridgman-Stockbarger method, binary halides, synthesis of the compound of the desired ammonia , crystallization and annealing, followed by cooling to room temperature by the Bridgman-Stockbarger method, and the synthesis and growth is combined in one quartz ampoule with a conical bottom, the synthesis is carried out by direct fusion of halides TlI, TlBr, Pb2, PbBr2 at a temperature of 870-890 K at a speed of 30 K / h, holding 6 hours, gradually reducing the temperature to room temperature. 20 K / h. |
priorityDate | 2016-10-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 16.