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filingDate 2001-03-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2005-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_18dfcd8e9580fd05ebd1491524bfb152
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publicationDate 2005-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber TW-I234568-B
titleOfInvention Preparation of rubber particles
abstract A process for preparing rubber particles K comprising in polymerized form (A) from 80 to 100% by weight, based on K, of one or more conjugated diene monomers A, and (B) from 0 to 20% by weight, based on K, of one or more monoethylenically unsaturated comonomers B by emulsion polymerization in the presence of an emulsifier and a polymerization initiator comprises (1) initially introducing a mixture M1 comprising water and emulsifier (2) adding a mixture M2 comprising, in monomeric or polymerized form, one or more monomers selected from styrene, alpha-methylstyrene, butadiene, n-butyl acrylate, methyl methacrylate and acrylonitrile, and, if appropriate, comonomers (3) starting the polymerization of the resulting mixture in the presence of a polymerization initiator at temperatures of from 5 to 95 DEG C, (4) adding a mixture M3 comprising from 0 to 100% by weight, based on B, of the comonomers B, and from 0 to 25% by weight, based on A, of the diene monomers A, (5) metering in a mixture M4 comprising the (remaining), diene monomers A, and the (remaining) comonomers B, and carrying out polymerization, and (6) ending the polymerization at a conversion above 90 and below 95%, based on the sum of the monomers.
priorityDate 2000-03-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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