http://rdf.ncbi.nlm.nih.gov/pubchem/patent/TW-201206950-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_598513b56c015a91156bee4e430b1b05 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-301 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-30 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-302 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07B61-00 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-30 |
filingDate | 2011-06-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_86545bec3969c02f307f1af43e4f0118 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a3c943a2b42ed2b1f2ec18cb7c7dbf9e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_33c019a0d547405e03fc715a98a1789a |
publicationDate | 2012-02-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | TW-201206950-A |
titleOfInvention | Method for producing N-substituted-2-amino-4-(hydroxymethylphosphinyl)-2- butenoic acid |
abstract | Provided is an effective synthesizing method of a (Z)-N-substituted-2-amino-4-(hydroxymethylphosphinyl)-2-butenoic acid derivative. A compound expressed by a next chemical formula (1) (chemical formula 1) where R1 represents a hydrogen atom or a C1-4 alkyl group, and a compound expressed by a next chemical formula (2) (chemical formula 2) H2N-COR2 (2) where R2 represents a C1-4 alkyl group, C1-4 alkoxy group, aryl group, aryloxy group or benzyloxy group, are dehydro-condensed in the presence or absence of an acid catalyst to synthesize a (Z)-N-substituted-2-amino-4-(hydroxymethylphosphinyl)-2-butenoic acid derivative; in where an organic solvent used for the reaction is a mixed solvent of an acetic acid and a solvent selected from a group consisted of a toluene, xylene and chlorobenzene, where a mixing ratio of the acetic acid and the toher solvent is 1: 3 to 1: 5 in volume, and in which the reaction is conducted by heating under reflux. |
priorityDate | 2010-06-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 72.