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filingDate 1977-11-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1981-01-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f187c56637743b08407e1a96ee28344c
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publicationDate 1981-01-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber SU-797581-A3
titleOfInvention Method of preparing aluminium ethylphosphite
abstract Prepn. of aluminium ethylphosphite comprises reaction of an excess of a ternary equilibrium mixt. of 23-93% of diethylphosphite, 59-7% of monoethylphosphite and 18-0.1% of phosphorous acid on opt hydrated alumina at 20-100 degrees C under reduced pressure, the water produced in the reaction being eliminated simultaneously. Process gives high yields and good reproducibility of product, used as a plant fungicide. Process is suitable for industrial scale. In a typical reaction, a mean yield of 96% was obtd. by reaction of a mixt. of 43% diethylphosphite, 49% of monoethylphosphite and 8% of phosphorous acid with alumina type H10 at 25-60 degrees C to give 95.2% aluminium ethylphosphite.
priorityDate 1976-11-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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