http://rdf.ncbi.nlm.nih.gov/pubchem/patent/SU-1520063-A1
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_7597492989bfbde2d72b8d592921a59d http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_4217861f08353f168e1595aa53974e0a http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_5028b8ca672fdc77986010a614f88110 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_c56a9d695bec7c4279938e70afd04c4c http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_daf0822bb4ac0ddc63cfbfbe32c78d36 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-80 |
filingDate | 1986-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1989-11-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_77f9abd60351fd9e11c5033dc24ddc28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_186d7793ec06b8953ae3c926f72d362a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d452022b3e0dc5257a5583dbe8e9777d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_670186df84cb7d8dd37fd0a5a392a2c2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_392dcf363c4d08b1d221405131fc1600 |
publicationDate | 1989-11-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | SU-1520063-A1 |
titleOfInvention | Method of obtaining diallyl esters of phthalic acids |
abstract | The invention relates to carboxylic esters, in particular to the preparation of diallyl phthalic acid esters, which are used in the manufacture of plastics. The goal is to increase the yield of the target product, reducing the consumption of raw materials and energy consumption. The esters are obtained by reacting alkali metal salts of these acids with allyl chloride at 40-50 ° C in the presence of copper monochloride and sodium bicarbonate using wastewater, which is obtained by displacing water from the stage of isolating the target product and its alkaline and water rinsing composition,%: sodium chloride 0.3-0.5n n n monoallylphthalate 1.6-2.0n n n phthalic acid 3.5-4.2n n n copper monochloride 0.26-0.35n n n water the rest. The process is followed by the additional introduction of sodium chloride to a content of 2.5-3.8 wt.%. The desired product is isolated by treating the reaction mass with isopropyl alcohol with a volume ratio of alcohol and organic phase of 1: 1. The consumption of allyl chloride is reduced by 30% with a yield of the target product of 99.6%. 2 ill., 2 tab. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2751105-C1 |
priorityDate | 1986-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 52.