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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N21-78
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D235-30
filingDate 1986-05-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1987-10-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_403aac5f68c0e36a42262eaf74135908
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_69a0ea67c7630a8b06f89333dc019188
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publicationDate 1987-10-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber SU-1342901-A1
titleOfInvention 1-(2ъ-oxy-5ъ-nitrophenyl)-3-isopropyl-5-(1ъъ-benzylbenzinidazolyl-2")formazan as selective reagent for spectrophotometric identification of cadmium,zinc,copper,mercury
abstract The invention relates to heterocyclic compounds, in particular to 1- (2 -oxy-5-nitrophenyl) -3-isopropyl-5- (1-benzylbenzimidazolyl-2) formazan as a selective reagent for spectrophotometric determination of Cd, Zn, Cu Hg Purpose -. obtaining new derivatives of the specified class with useful properties. Formazan is prepared from 1-benzylbenzimidazolyl-2-hydrazone of isobutyraldehyde in isopropyl alcohol and diazo solution prepared from 2-amino-4-nitrophenol, concentrated HC1 and NaNO1), while cooling in an acidic medium. The mixture is basified with NaOH to pH 8-9, then adjusted to neutral. Yield 65%, mp. 136-138 ° C. Tests show that formazan, along with the property of selective complexation with Cd, Zn, Cu Hg ions, has the ability to form these complexes in different pH ranges of the medium, which makes it possible to determine these elements without prior separation. 2 ill., 2 tab. f (L
priorityDate 1986-05-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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