http://rdf.ncbi.nlm.nih.gov/pubchem/patent/SU-1293640-A1
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_febb4b887e6362a447f36aff9cc6de5f http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_812446bf0f826ba71a5c47f6cf796485 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_6b7b6068e5fe9bfedf828d2eaec57622 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-00 |
filingDate | 1985-10-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1987-02-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_62f1fe0c35a55dad01aa2cc120e02d85 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_70c487c4192fcccb67c30ce143992d9e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_22e3495364fc53065554b21e53f9c12f |
publicationDate | 1987-02-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | SU-1293640-A1 |
titleOfInvention | Method of determining composition of reaction mixture for synthesizing cyclohexyl chloride from cyclohexane |
abstract | This invention relates to analytical chemistry, in particular, to determining the composition of the reaction mixture (CPC) for the synthesis of cyclohexyl chloride from cyclohexane. An increase in the accuracy of the analysis is achieved by using a carrier in a column with a varying content of tricresyl phosphate applied on it from 18–22 wt.% At the inlet of the column to 3–7 wt.% At its output. The determination of CPC is carried out by dividing the analyzed sample on a column with the indicated carrier with a gradual increase in the temperature of the column at a speed of 6-12 sec / min, starting from an initial temperature of 45-55 ° C. The separated components are subjected to detection. The accuracy obtained in the method of analyzing the components of the CPC is, wt.%: Cyclohexane ± 4, cyclohexene t9.5, cyclohexyl chloride 0.5, dichlorocyclohexene t2, against 19.5, 9.5, O and 36 in the known case. 2 tab. with (L yu od od 4ii |
priorityDate | 1985-10-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 33.